Gelation Threshold Calculator

Model gel formation using functionality and conversion. Compare predicted gel point against your target window. Plan experiments confidently with clear outputs and exports included.

Calculator

Tip: Start with mixture mode for multi-monomer systems.
Choose direct entry or compute average functionality from a formulation table.
Optional. If blank, only p_c is calculated.
Must be greater than 1 to form an infinite network.
Mixture definition
Enter each component’s functionality and fraction (mole fraction, mass fraction, or any consistent fraction).
Component name Functionality (f) Fraction (x) Remove
Fractions will be normalized if they do not sum to 1.

Formula Used

This calculator uses a common step-growth gelation approximation based on average functionality:

Critical conversion (gel point)
pc = 1 / (favg − 1)
  • favg is the average functionality of reactive species.
  • p is the extent of reaction (conversion), from 0 to 1.
  • If p ≥ pc, gelation is likely (network forms).

Assumptions: random branching, equal reactivity, and no strong intramolecular cyclization effects. Real systems may deviate; validate with rheology or sol–gel testing.

How to Use This Calculator

  1. Choose Direct f_avg if you already know average functionality.
  2. Choose Mixture to compute favg from your formulation.
  3. Optionally enter conversion p as a fraction or percent.
  4. Press Submit to see results above the form.
  5. Use Download CSV or Download PDF to export.

Tip: If your conversion is uncertain, run multiple values to map a safe window below pc.

Example Data Table

Scenario f_avg p (conversion) p_c Interpretation
Mostly bifunctional with small brancher 2.40 0.30 0.7143 Below gel point; mixture remains a sol.
Higher branching 3.00 0.55 0.5000 At/above gel point; gel network likely forms.
Near-threshold design check 2.80 0.45 0.5556 Safety margin remains; monitor conversion drift.
Numbers are illustrative for planning and training.

Gelation threshold and processing signals

Gelation threshold marks the shift from finite clusters to a sample-spanning network in step-growth and sol–gel systems. Near this point, viscosity climbs rapidly, elastic response appears, and filtration or pumping becomes difficult. Using a calculated critical conversion p_c gives a practical “do not cross” marker for pot life and processing. Track temperature, catalyst level, and residence time because each can accelerate conversion toward the threshold.

Average functionality as a formulation lever

Average functionality f_avg summarizes how many reactive connections molecules can form on average. Adding trifunctional or tetrafunctional branchers raises f_avg and lowers p_c, so gelation occurs earlier. Monofunctional stoppers and excess difunctional content reduce f_avg and delay network formation. In mixture mode, weight or mole fractions must be consistent; the calculator normalizes fractions to prevent arithmetic bias when inputs do not sum to one.

Interpreting p versus p_c for control

Conversion p represents the fraction of functional groups that have reacted. Compare measured p from titration, spectroscopy, or calorimetry to p_c to interpret batch status. If p is well below p_c, the material should remain a sol with manageable flow. As p approaches p_c, small errors in measurement matter; sampling delays can push p over the line, triggering gel and trapping bubbles or fillers.

Sensitivity checks for robust decisions

Sensitivity checks strengthen decision making. Recompute p_c using plausible ranges for f_avg based on supplier specs, moisture uptake, and equivalent-weight uncertainty. For formulations, vary brancher fraction and observe how strongly p_c moves; large shifts indicate a narrow processing window. Use the margin p_c − p to set control limits, choose sampling frequency, and define maximum hold times. When scaling, account for heat removal differences that raise reaction rate. If you target a specific gel time, adjust catalyst or temperature so predicted p remains below p_c during mixing, then crosses p_c only after application or molding with checks at each stage.

Model limits and validation pathways

This relation is a screening model that assumes random branching, equal reactivity, and minimal cyclization. Real systems may gel later or earlier due to intramolecular loops, phase separation, diffusion limits, or unequal rate constants. Validate the estimate with rheology (G′/G″ crossover), gel content, or solubility tests at your cure schedule. Use the calculator to compare scenarios, document assumptions, and communicate risk across R&D, production, and quality teams.

FAQs

What is gelation threshold in this calculator?
It is the predicted critical conversion p_c where an infinite network becomes likely under step-growth assumptions. Below p_c the system is typically a sol; at or above p_c gel formation is expected.
How do I choose direct versus mixture mode?
Use direct mode when you already know f_avg from characterization or a validated model. Use mixture mode when you need f_avg from multiple components using their functionalities and formulation fractions.
Do the fractions need to sum to one?
No. You can enter any consistent fractions. The calculator normalizes them internally so the effective fractions sum to one before computing the weighted average functionality.
What conversion value should I enter?
Enter the extent of reaction p as a fraction (0–1) or percent. If you do not have p, leave it blank to compute only p_c and use it as a target limit during processing.
Why does p_c cap at 1.00?
Conversion cannot exceed 1.00 in the usual definition. If the formula predicts a value above one, it implies gelation is not expected within full conversion for that low f_avg case.
How can I validate the prediction experimentally?
Confirm with rheology, gel content, or solubility testing at your cure schedule. Track G′/G″ crossover or insoluble fraction near the predicted p_c, and refine f_avg inputs based on observed behavior.

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Important Note: All the Calculators listed in this site are for educational purpose only and we do not guarentee the accuracy of results. Please do consult with other sources as well.